Synovex
Important Note:
Be Sure To See Why
Show-Tech TM
Is The Best Choice For
Alternative Steroid Supplements Ever!
Cattle implants are an easy way for the average guy to get his hands on some of the good stuff. Trenbolone acetate is the most popular of this form of steroid as it easily separated from Finaplix or Component pellets. It is usually made into an injectable or topical doseage form. Synovex-H is a lesser known implant that contains 2 grams of testosterone propionate (TP) and, unfortunately, 200mg of estradiol benzoate (EB) per cartridge. Synovex is even more readily available than Fina, and can be found with a simple internet search. No proof of cattle ownership is usually needed, and 20g of testosterone propionate can be had for as little as $70.
There are several ways to remove the estradiol that are commonly known. One involves using diethyl ether and a freezer, and another involves removing the esters before separating. The former method does not completely remove the estradiol, and the latter is bad because the pharmokinetics of straight testosterone in oil are less than desirable (the free base is better for transdermal preparations, however, and will be covered later). Ideally, we could remove the esterified testosterone, without the estrogen.
Good news! I’m going to explain, step by step, how to separate pure testosterone propionate from the estradiol benzoate. The technique is basically a recrystallization of a supersaturated solution, which is commonly used in chemistry to purify substances. I will go through the method with the approximate amounts of chemicals needed to do one cart of Synovex-H. One cart refers to one green cartridge, which is a green cylinder full of pellets, and all together contains 2 grams of TP and 200mg of EB. The actual amounts of chemicals will vary every time you do the procedure, because variables such as temperature and atmospheric pressure are never the same all the time.
Recrystallization
Materials needed: Methanol (Heet) -- The amount needed will vary with the number of recrystallizations. Distilled water, 2 glass containers (Jars preferably), a 60ml syringe, syringe prefilter (.8 to 1.2 micron) and coffee filters.
Note: Be sure to get regular Heet in the yellow bottle. Read the label and use it if it contains ONLY methyl alcohol, and only methyl alcohol.
The Theory (a.k.a how the hell does this work?)
In this method, we take advantage of the fact that there is ten times more testosterone propionate than estradiol benzoate in the cartridge. Both TP and EB are freely soluble in methanol and almost completely insoluble in water. As detailed in Weissberger's "Technique of Organic Chemistry Volume III, Part I Separation and Purification." (1), by slowly adding distilled water to the methanol/steroid solution, we can create a supersaturated solution. This supersaturated solution will crystallize; giving highly pure crystals of the substance that was supersaturated in the solution. Since there is ten times more TP than EB, the solution becomes saturated with TP first, so it will crystallize first. The crystals that form will be pure, but all of the TP will not come out of solution when the first crystals form. Only enough TP will crystallize so that the remaining TP in solution will not be extremely supersaturated. For example, if 200mg TP crystallizes, 1800mg will still be in solution per cart. The one thing to be aware of is that after a certain amount of water is added, the EB will become supersaturated and crystallize as well. The only way to know for sure if there is estrogen in your crystals will be to do take a melting point of some of the crystals.
The Nitty Gritty
Dissolve the cart in 80mls of methanol. This will take about an hour. I put everything in a jar and shake it up. Also, crushing the pellets after about 15 minutes of soaking speeds up the process. Let the filler settle on the bottom of the jar. Use a 60ml syringe to draw up the liquid above the filler that has settled on the bottom. You can leave most of the filler at the bottom, as it is a mess to filter.
Put the syringe filter on and filter the solution into a new, clean, dry jar. The solution should be clear. Now we begin adding the distilled water. The water should be added slowly, and when opalescence is seen in the solution, the water should stop being added, because crystallization is occurring. The whole solution needs to be cloudy before crystallization will really occur, do not confuse this with the cloudiness that happens right where the water hits the methanol. Once the solution is cloudy, screw the cap on the jar and let it sit for at least a half hour. The amount of water that you need to add to get crystals is about 13-25 ml. Be sure to add the water slowly after 10 ml or so. Be patient, because the slower that the crystals form, the more pure they are.
Once the crystals have formed, you want to harvest them. Place a coffee filter in the mouth of another clean, dry jar, so that the crystals can be filtered. Swirl the solutions before you pour it to make sure you get all the crystals. Squeeze the excess liquid through the filter. Once the solution is completely through the filter, remove the filter, label it as the 1st crop, and set it aside. This process is then repeated. Water is added to the solution we just filtered until it is cloudy. Seal the jar and let it crystallize, and harvest the crystals. Be sure to label each crop of crystals -- the number of crops needed will vary.
Once all the crystals are harvested, and allowed to dry overnight, it is time to process them. A melting point will be needed for each crop of crystals. The melting point of TP is 120-122 C (248-251.6 F). If estrogen is present, the melting point of the crystals will be lower than this. Our goal is to get the melting point to 120 C (248 F). Most likely all of the first crops of crystals will have some estrogen in them. This is where the procedure gets a little complicated, but if you can do this, you will be successful. To get really pure crystals, just enough methanol is added to each crop of crystals so that all the crystals are dissolved. Water is added drop wise to these solutions until crystals form, just as we did previously. The crystals are harvested, and melting points are taken. It usually only takes a few simple recrystallizations to get a really pure product. The yield will vary each time you try this, but I recommend just doing one cart at a time, until you get the hang of it.
There are many ways to measure melting point, but an easy way to do it at home is to put some about oil in a pan on a stovetop burner. You will need an accurate thermometer, a test tube, and a few milligrams of your crystals. Be sure you can easily tell the difference between 115 C (239 F) and 120 C (248 F) degrees, this small difference is important! Turn on the burner and heat it to about 100 C (212 F). Make sure the temp is stable. Now put the crystals in the test tube and hold this in the oil, but do not let the test tube touch the bottom of the pan. Slowly increase the heat until the crystals melt, and note the temperature. When the crystals melt at 118 C - 120 C (244.4 F - 248 F), you have pure testosterone propionate.
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There is overwhelming evidence which shows that creatine supplementation does cause an increase in the amount of creatine phosphate in muscles. Harris et al (1992) conducted a study examining creatine content in the quadriceps femoris muscle in 17 subjects after supplementation of 5 g of creative monohydrate 4-6 times a day for two days. The results found a significant increase in the total creatine level in all subjects but the results were especially noticeable in those with the lowest muscle creatine store at the start of the study. To determine whether exercise could affect the amount of creatine absorbed by muscles, some of the participants followed a unique training program. During supplementation, they pedaled a bicycle ergometer for one hour each day while using only one leg to supply the pedaling force. With supplementation, the unexercised legs increased their creatine levels by about 25 percent, but the exercised legs increased their creatine levels by 37 percent. It is hypothesized that exercise increases the flow of blood to the muscles or changes the rate at which muscles absorb creative from the blood, thus improving the creatine loading effect. Another study conducted by Febbraio replicated the results obtained by Harris.
Several studies also show that creatine supplementation does cause an increase in muscle strength. Earnest et al (1995) conducted a study investigating the influence of creatine monohydrate supplementation on muscular power and strength in 10 experienced weight trained male subjects. Three series of high intensity, anaerobic type muscular workouts were used. The first series consisted of three consecutive 30 second Wingate bike tests, followed by five minuets of rest. Peak anaerobic power was defined as the greatest power achieved in a given five second work interval. Anaerobic work was defined as the total amount of work performed in a 30 second period. The second series used a one repetition maximum (lRM) free weight bench press as a test of muscular strength. The third series utilized complete lifting repetitions at 70% of the bench press IRM until fatigue. Fatigue was defined as the inability to complete one lifting repetition or the inability to maintain a lifting cadence of one second eccentric and one second concentric (lifting and lowering the weight). Total lifting volume was calculated as 70% of pre-test IRM multiplied by the number of complete lifting repetitions. Subjects received either a glucose placebo or creatine monohydrate supplement in a double blind fashion. (After 14 days of supplementation, each subject was re-tested on the Wingate bike tests. Re-testing for the weight lifting trials was done after 28 days of supplementation.
Within the creatine group, total anaerobic work from the Wingate tests was significantly higher during all post-test trials. The increases were 13% for series one, 18% for series two and 18% for series three. No changes were noted in the placebo group. Greater total anaerobic work resulted from the creatine subject's ability to achieve and maintain higher levels of anaerobic power consistently over- each five second time interval. Bench press IRM increased 6% in the creatine group. Total lifting volume was significantly higher within the creatine group, whether expressed in absolute terms (26%) or relative terms (29%). Increases in the total lifting volume were associated with the ability of the creatine group to perform 26% more lifting repetitions. The authors conclude that the ability of the creatine group to perform a greater total lifting volume demonstrates the effectiveness of creatine as an ergogenic aid.
In Hultman's study (cited in Anderson, 1974) these results were replicated. Each day, creatine was given in six separate doses of five grams a day. During the six-day period, five other Estonian runners of comparable ability received a glucose placebo instead. All runners were unaware of the actual composition of their supplements. Before and after the six-day supplementation, the athletes ran four 300-meter and (on a separate day) four 1000-meter intervals, with three minutes of rest between the 300-meter intervals and four minutes of rest between the 1000-meter intervals. Improvement on the final 300-meter interval (from pre-to-post supplementation) was more than twice as great for creatine users, and improvement was more than three times as great for creatine supplements in the final 1000-meter interval. Total time to run all four 1000-meter intervals improved from 770 to 757 seconds after creatine supplementation. In comparison, the placebo group actually slowed from 774 to 775 seconds.
In Hultman's study (cited by Anderson, 1994) creatine supplementation was very important during the last interval of each workout. Creatine supplementers doubled their advantage during the final 300-meter interval and tripled their advantage in the closing 1000-meter sprint. This supports Hultman's hypothesis that creatine is likely to be most helpful when lactic acid levels are highest and fatigue is greatest. Hultman thus feels that creatine serves as a buffer lowering lactic acid muscle burn and delaying fatigue, thus allowing an athlete to perform longer workouts.
In contrast, Balsom at al (1993) investigated the influence of creatine supplementation on endurance exercise performance in the form of a 6 km run and showed that creatine supplementation does not enhance performance or increase peak oxygen uptake during prolonged continuous exercise. There was actually decreased performance in the creatine supplementation group, which may be attributed to the participants weight gain.
In support of Balsam et al (1993), Febbraio et al (1995) conclude that creatine supplementation "may not increase performance during exercise where a significant proportion of energy is derived form aerobic metabolism." This aerobic metabolism occurs during more prolonged, sustained exercise as opposed to anaerobic metabolism which occurs during fast, nonsustained muscle contractions. It is therefore more likely that if creatine supplementation has an effect it will only be seen during brief, anaerobic exercise such as sprinting or weight lifting.
As you may or may not know, creatine monohydrate will not fully dissolve in liquid. That's why you always get that gritty sand at the bottom of the glass. Look at it this way, if it falls like sand to the bottom of your glass what does it do in your stomach? Maybe that explains why so many complain of stomach discomfort when using regular creatine monohydrate.
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Faster Absorption
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More Efficient
20 times more total surface area for greater uptake into the bloodstream.
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Micronizing creatine produces a more pure creatine. By increasing the total processing steps and purification procedures, "CreaBlast" yields a finished product substantially more pure. Test it. We challenge you.
Mixes Easier and Better
"CreaBlast" Creatine has 20 times more surface area. Greater service area means easier, faster and more complete mixing.
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Regular creatine monohydrate sits in the gut longer. This causes discomfort to many users. CreaBlast Micronized Creatine goes into solution better and leaves the gut quicker causing no stomach upset.
Better Results
New "CreaBlast" Micron High grade Creatine offers 2000% more particle surface area for better utilization, better uptake, and faster results.
Drink Plenty of Liquids!
Creatine works by enhancing muscle cell hydration. It is very important to consume adequate fluids while taking creatine to see best results. A good rule of thumb is to drink an EXTRA 16 to 20 ounces of liquid for every 5 grams of creatine you take.
During your Loading Phase you should be drinking an EXTRA 64 to 80 ounces of liquid than you normally drink. During the maintenance phase you should drink an EXTRA 32 to 40 ounces.
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